Experimental an theoretical studies on the improved application of displacement washing for cracked filter cakes

IGF Project No. 01IF23518N


Background

Cake filtration is a flexible, generally well-controllable, and relatively cost-effective technology for solid-liquid separation. In many cases, on-spec separation result regarding soluble components can only be achieved through additional displacement washing, during which the wash liquid penetrates the surface of the filter cake and displaces the pore liquid. The standard preliminary tests for the subsequent design of industrial filtration systems are typically conducted for this purpose in small laboratory setups under defined conditions.

Process Challenges: Cracking

In actual industrial processes, crack formation frequently occurs in the filter cake (for example, due to partial desaturation leading to shrinkage processes). Such filter cakes typically elude standardized laboratory methodologies because the cracks occur stochastically with regard to their size, shape, and distribution. Since cracks exhibit a significantly lower flow resistance, the wash liquid preferentially flows through these defects, bypassing the actual filter cake. The process engineering consequences of this bypass flow (channeling) are uncertain plant designs, highly heterogeneous washing, an increased demand for wash liquid, as well as an undesirable dilution of the filtrate. To date, there is a lack of quantitative fundamental knowledge to evaluate the process engineering impacts of cracks. This is the starting point for the current research project.

Research Approach and Methodology

Contrary to the conventional approach of simply trying to prevent cracks in advance, this project establishes an understanding of the effects of existing cracks and develops strategies to mitigate these impacts. As a first step, a method is being developed to create reproducible, geometrically defined cracks within a filter cake. The effects of various crack geometries are then investigated experimentally in laboratory nutsche filters, qualitatively through dye tests and quantitatively through washing experiments. In parallel, theoretical modeling is performed in COMSOL, which is validated or revised based on the experimental findings.

Initial dye tests already show a clear picture. In the following figures, a flat filter cake (without a crack) can be seen on the left, and a filter cake with an artificially created crack is shown on the right. For the washing process, the wash liquid was dyed with blue food coloring to make its flow paths visible. It is clearly evident that the flow influenced by the crack (bypass flow) is less efficient and that the crack flanks are only poorly permeated (cake height: 3 cm, pressure difference: 0.5 mbar, wash ratio: 0.33).

First simulations are consistent with the results of the dye tests. For a flat filter cake, the flow of the wash liquid through the filter cake is shown below:

In contrast, a cracked filter cake presents a significantly different flow profile:

Practical Transfer and Industrial Benefits

To verify the transferability of the laboratory findings to the pilot scale, experimental investigations will be conducted on an indexing belt filter (0.1 m²) in the further course of the project. Building upon this, comprehensive strategies to mitigate the impacts of cracks will be developed, such as modifying the wash water application or partially resuspending the cake layer. With these new findings, companies acting as planners, manufacturers, or operators along the value chain will be able to design filter systems and operations more safely, rapidly, and resource-efficiently in the future.

The IGF Project No. 01IF23518N of the research association Forschungs-Gesellschaft Verfahrens-Technik e.V., Theodor-Heuss-Allee 25, 60486 Frankfurt am Main, was funded by the Federal Ministry for Economic Affairs and Climate Action within the framework of the “Industrial Collective Research (IGF)” program, on the basis of a decision by the German Bundestag.

Last updated: 30.07.2026

Contacts

Prof. Dr. Bernhard Hoffner
+49 621 292-6306
b.hoffner@th-mannheim.de

M. Sc. Peter Hartmann
+49 621 292-6303
p.hartmann@th-mannheim.de

M. Sc. Nico Lützel
+49 621 292-6303
n.luetzel@th-mannheim.de

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